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Beilstein J. Org. Chem. 2017, 13, 995–1007, doi:10.3762/bjoc.13.99
Graphical Abstract
Figure 1: Chemical structure of PC-C18pPhC18-PC.
Scheme 1: Synthesis of PC-C18pPhC18-PC; TBAF: tetra-n-butylammonium fluoride, TEA: triethylamine, rt: room te...
Figure 2: DSC curves for PC-C18pPhC18-PC (c = 1 mg mL−1 in H2O, solid lines, heating: red, cooling: blue). FT...
Figure 3: TEM image of an aqueous suspension (c = 0.05 mg mL−1) of PC-C18pPhC18-PC. The samples were prepared...
Figure 4: SANS data of a suspension of PC-C18pPhC18-PC (c = 1 mg mL−1 in D2O, scattered data) with IFT analys...
Figure 5: DSC heating (left-hand column) and cooling (right-hand column) scans of different PC-C18pPhC18-PC:p...
Figure 6: TEM images of aqueous suspensions (c = 60 µM or c = 30 µM for C) of PC-C18pPhC18-PC/phospholipid mi...
Figure 7: FTIR spectroscopic data (symmetric CH2 stretching vibration: red squares, right axis; symmetric CD2...
Figure 8: (A) SAXS diffractograms of an equimolar mixture of PC-C18pPhC18-PC/DPPC (c = 10 mg mL−1, scattered ...
Beilstein J. Org. Chem. 2017, 13, 938–951, doi:10.3762/bjoc.13.95
Figure 1: Interaction of a shape-persistent CD polymer with ditopic guests.
Figure 2: Schematic representation of tip and surface modifications realized in this study (bottom). Blue lin...
Scheme 1: Synthesis of the CD polymer. a) conc. HNO3, reflux, 6 d; b) tert-butanol, cat. H2SO4, MgSO4, CH2Cl2...
Figure 3: Absorption spectra of monomer 7 (solid red line) and polymer 8 (solid blue line) in water. Emission...
Figure 4: Positive linear MALDI–TOF spectrum of polymer 8 using HABA/TMG2 matrix.
Figure 5: SANS data for polymer 8 and fit by cylindrical model (solid line).
Scheme 2: Ditopic and monotopic guest molecules.
Figure 6: Solubility of polymer 8 in the presence of ditopic connector 9 (black graph) and 1-aminoadamantane ...
Scheme 3: Synthesis of amino functionalized polymer 12.
Figure 7: Characteristic force curves recorded during retraction of the AFM tip from the surface. Four functi...
Figure 8: Graphical summary of experimental results for the four configurations of CD attachment introduced i...
Figure 9: (a) Detail of the end of a force curve for a polymer-functionalized tip retracted from a polymer-fu...
Figure 10: Characteristic result of a friction experiment for a polymer-functionalized tip sliding on a surfac...